Mahsulotni tanishtirish
| 2,3-Lutidine Basic ma'lumotlari |
| Mahsulot nomi: | 2,3-Lutidin |
| Sinonimlar: | 2,3-DIMETHYLPİRIDIN(2,3-LUTIDINE);a,b-Dimetilpiridin;2,3-Lutidin (8CI);Piridin, 2,3-dimetil-(9CI) );2,3-Lutidin, 98+% 100ML;2,3- ikkiMetilpiridin;2,3-Lutidin 99%;LUT |
| CAS: | 583-61-9 |
| MF: | C7H9N |
| MVt: | 107.15 |
| EINECS: | 209-514-1 |
| Mahsulot toifalari: | Biokimyo;Oligosakkaridlar sintezi uchun reagentlar;Piridin hosilalari;Heterotsiklik birikmalar;bc0001 |
| Mol fayli: | 583-61-9.mol |
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| 2,3-Lutidinning kimyoviy xossalari |
| Erish nuqtasi | -15 daraja (lit.) |
| Qaynash nuqtasi | 162-163 daraja (lit.) |
| zichligi | 0.945 g/ml 25 daraja (lit.) |
| sindirish ko'rsatkichi | n20/D 1.508 (lit.) |
| Fp | 122 daraja F |
| saqlash harorati. | Inert atmosfera, Xona harorati |
| pka | 6,57 (25 daraja) |
| shakl | Suyuqlik |
| rang | Shaffof rangsizdan biroz sariq ranggacha |
| Suvda eruvchanligi | 95 g/L (26 ºC) |
| BRN | 106418 |
| InChIKey | HPYNZHMRTTWQTB-UHFFFAOYSA-N |
| TABASS | CC1=C(N=CC=C1)C |
| LogP | 1,638 (taxminiy) |
| CAS ma'lumotlar bazasiga havola | 583-61-9(CAS ma'lumotlar bazasi ma'lumotnomasi) |
| NIST kimyo ma'lumotnomasi | Piridin, 2,3-dimetil-(583-61-9) |
| EPA moddalarni ro'yxatga olish tizimi | 2,3-Dimetilpiridin (583-61-9) |
| Xavfsizlik ma'lumotlari |
| Xavf kodlari | Xn, F, Xi |
| Xavf bayonotlari | 10-22-37/38-41-20/21/22-36/37/38 |
| Xavfsizlik bayonotlari | 16-26-39-36/37-36/37/39 |
| RIDADR | BMT 1993 3/PG 3 |
| WGK Germaniya | 3 |
| TSCA | Ha |
| HazardClass | 6.1 |
| PackingGroup | II |
| HS kodi | 29333990 |
| MSDS ma'lumotlari |
| Provayder | Til |
|---|---|
| 2,3-Dimetilpiridin | Ingliz |
| SigmaAldrich | Ingliz |
| ACROS | Ingliz |
| ALFA | Ingliz |
| 2,3-Lutidindan foydalanish va sintez |
| Tavsif | 2,3-Lutidin piridin hosilalari guruhiga mansub boʻlib, organik sintezda oraliq mahsulot va kislotani bogʻlovchi vosita sifatida ishlatiladigan, sotiladigan organik reagentdir. Bundan tashqari, lazzatlanish uchun oziq-ovqat qo'shimchasi sifatida ishlatiladi. |
| Kimyoviy xossalari | tiniq rangsiz yoki bir oz sariq suyuqlik |
| Foydalanadi | 2,3-Lutidin lansoprazol oraliq mahsulotidir. U farmatsevtika oraliq mahsuloti sifatida ishlatiladi. |
| Ta'rif | LOTUS: 2,3-Lutidin - bu Nicotiana tabacumda mavjud ma'lumotlarga ega tabiiy mahsulot. |
| Sintez uchun havola(lar) | Organik kimyo jurnali, 66, p. 53, 2001 yilDOI:10.1021/jo000724t |
| Tozalash usullari | Taxminan 20% H2SO4 ning 1,2 ekvivalentini o'z ichiga olgan eritmadan bug' bilan distillanadi, toki asosning taxminan 10% asosiy bo'lmagan aralashmalar bilan o'tadi. Keyin kislotali eritma ishqoriy holga keltiriladi va asos ajratiladi, NaOH yoki BaO ustida quritiladi va qisman distillanadi. Distillangan lutidin 100 g ni 40 g karbamid bilan 75 ml H2O ga aralashtirish, 5 o ga sovutish, nasosda filtrlash va 75 ml H2O bilan yuvish orqali o‘zining karbamid kompleksiga aylanadi. 300 ml H2O da eritilgan kompleks distillat ozgina qattiq NaOH bilan loyqalik bermaguncha bug'da distillanadi. Keyin distillat ortiqcha qattiq NaOH bilan ishlanadi va yuqori qatlam chiqariladi: keyin suvli qatlam dietil efir bilan chiqariladi. Yuqori qatlam va efir ekstrakti birlashtiriladi, quritiladi (K2CO3) va qisqa ustun orqali distillanadi. Yakuniy tozalash qisman muzlatish yordamida fraksiyonel kristallanish orqali amalga oshiriladi. Pikrat EtOH dan m 187-188o bilan kristallanadi. [Kyte va boshqalar. J Chem Soc 4454 1960, Beilstein 20 H 243, 20 II 159, 20 III/IV 2765, 20/6 V 15.] |
| 2,3-Lutidin tayyorlash mahsulotlari va xomashyo |
| Xomashyo | 2,3,4-trimethylpyridine-->Pyridine, 1,2,3,4-tetrahydro-5,6-dimethyl--->(2-Methylpyridin-3-yl)methyl acetate-->Ethanone, 1-(1-methyl-3-piperidinyl)- (9CI)-->2,3,6-TRIMETHYLPYRIDINE-->(2-METHYL-PYRIDIN-3-YL)-METHANOL-->3-Ethylpyridine-->Etil 2-metilnikotinat |
| Tayyorlash mahsulotlari | 2-Chloromethyl-3-methyl-4-(2,2,2-trifluoroethoxy)pyridine hydrochloride-->3-METHYL-2-PYRIDINECARBOXALDEHYDE-->2-HYDROXYMETHYL-3-METHYLPYRIDINE-->2,3-DIMETHYL-PYRIDIN-4-YLAMINE-->2-Chloromethyl-3-methyl-4-(3-methoxypropoxy)pyridine hydrochloride-->4-Chloro-2,3-dimethylpyridine 1-oxide-->Lansoprazole-->2-HYDROXYMETHYL-4-METHOXYPROPOXY-3-METHYLPYRIDINE-->4-Nitro-2,3-lutidine-N-oxide-->2,3-Dimethylpyridine-N-oxide-->2,6-Lutidine-->Piridin |
Issiq teglar: 2,3-lutidin, Xitoy 2,3-lutidin ishlab chiqaruvchilari, yetkazib beruvchilari, zavodi
Oldingi: 3,5-Lutidin
Keyingi2: 4-Sianopiridin
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